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target="_blank">计量校准</a>校验方法<br /> 1 .锤的落距和击实筒高度用钢直尺测量。 2. 用游标卡尺测量锤底和击实筒直径，分别在互相垂直的两个方法测量，取算术平均值。 3． 用天平称量锤的质量。 4.校验结果处理 全部校验项目均符合技术要求为合格。 5校验周期 校验周期为12个月。 <br /> <br /> <div> 光电式液、塑限测定仪校验方法 本方法适用于新购和使用中及检修后的光电式液、塑限测定仪（光电式液、塑限联合测定仪）的校验。 <br /> 一、技术要求 1．1 锥体在吸附断电后，可自由下落，且不得有旷动。 1．2 锥体部分的总质量为76±0.2g。 1． 锥体夹角为0±0.2°。 1．4 锥尖容许磨耗不得大于0.mm。 <br /> 二、校验项目及条件 2．1 校验收项目 2．1．1 锥体吸附断电后下落情况。 2．1．2 锥体部技术参数： ①锥体质量。 ②锥体夹角。 ③锥尖磨耗。 2．2 校验用器具 2．2．1 天平：称量200g，感量0.1g。 2．2．2 游标卡尺：量程00mm，分度值0.02mm。 <br /> 三、校验方法 ．1 用目测检查断电后锥体下落情况。 ．2 用天平称量锥体质量，准确至0.1g。 ． 用游标卡尺测量锥底直径和锥高后，计算出锥尖夹角，准确至0.1°。4 用游标卡尺测量锥尖磨耗，准确至0.1mm。 四、校验结果处理 全部校验项目均符合技术要求为合格。 五、校验周期 校验周期为12个月。 <br /> <br /> 灌砂仪校验方法 本方法适用于新购和使用中及修理后的灌砂仪的校验。</div> <div> 说到这儿，可能有人要问了，有没有更直接点的做法呢，毕竟光说原理，对于小白来说，还是不知道怎么做。先说定量限：首先，配制一个较低浓度的对照品溶液，注入液相色谱仪，观察其峰高比基线噪音高多少倍（假设X倍），将该溶液稀释到X/倍，基本即为该物质的检测限，将该溶液稀释到X/10倍，基本即为该物质的定量限</div> <div> 再说检测限：您先做标准曲线，然后把低浓度点的标准品不断稀释进样，直到低的仪器能准确定量的点，然后连续进样7针（更大的奇数针），然后算出标准偏差，然后乘以，除以您做的标准曲线的斜率，就得到仪器的检测限。方法检测限是拿<a href="http://www.nbw1688.com" 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