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class="info"><span>让需要校准、检测、检定的地方都有博计计量</span> <a href="http://wpa.qq.com/msgrd?v=3&uin=1455914156&site=qq&menu=yes" target="_blank"><img alt="qq" src="https://www.nbw1688.com/static/images/qq.gif"/>[在线咨询]</a> <small>时间:</small>2021-06-11</div> </div> <div class="con clearfix"> <p>大型检测仪检定方法</p><p><a href="http://www.nbw1688.com" target="_blank">计量校准</a>基于不同物质具有不同的热导系数，几乎对所有VOCs都有响应，可以检测各种VOCs，且样品不被破坏，但灵敏度相对较低。</p><p>氢火焰离子化检测器（FID）：利用有机物在氢火焰的作用下化学电离而形成离子流，借测定离子流强度进行检测。 检测时样品被破坏，一般只能检测那些在氢火焰中燃烧产生大量碳正离子的有机化合物。</p><p>电子捕获检测器（ECD）：利用电负性物质捕获电子的能力，通过测定电子流进行检测。ECD具有灵敏度高、选择性好，是目前分析痕量电负性有机化合物有效的检测器。</p><p>火焰光度检测器（FPD）：对含硫和含磷的化合物有比较高的灵敏度和选择性，当含磷和含硫物质在富氢火焰中燃烧时，分别发射具有特征的光谱，透过干涉滤光片，用光电倍增管测量特征光的强度。</p><p>质谱检测器（MSD）：采用高速电子撞击气态分子或原子，将电离后的正离子加速导入质量分析器中，按质荷比（m/z）的大小顺序进行收集和记录，是一种质量型、通用型检测器。</p><p>在计量所不能对专业的大型检测仪器进行检定的情况下，由仪器工程师进行校准。</p><p>4.2.4 对检测仪器，每年进行一次全面保养维护和校准。 </p><p>4.2.5 对大型分析仪器，有设备责任人联系仪器工程师校准。在进行校正或校准前，对仪器进行全面的、系统的保养，包括对光路、采样针、样品轨道、各机械运动进行检查、校正，然后使用校准物对仪器进行校准，并验证。由工程师出具仪器检修校准报告，以明确仪器运转良好。 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